水热辅助相转移催化水解十二烷基苄氯的研究
发布时间：2018-07-25 11:50
【摘要】：采用超声、微波、水热、相转移催化等多种方法对n-十二烷基苄氯的碱性水解反应进行初步尝试,其中相转移催化与水热条件偶合水解获得了成功。优化的工艺条件为:十二烷基二甲基苄基氯化铵为相转移催化剂,在130℃下碱性水热反应16 h,此条件下n-十二烷基苄醇的产率达到93.6%。
[Abstract]:The alkaline hydrolysis of n-dodecyl benzyl chloride was studied by ultrasonic, microwave, hydrothermal and phase transfer catalysis, among which the coupling hydrolysis of n-dodecyl benzyl chloride with hydrothermal conditions was successful. The optimum process conditions were as follows: dodecyl dimethyl benzyl ammonium chloride as phase transfer catalyst, alkaline hydrothermal reaction at 130 鈩，
本文编号：2143734
[Abstract]:The alkaline hydrolysis of n-dodecyl benzyl chloride was studied by ultrasonic, microwave, hydrothermal and phase transfer catalysis, among which the coupling hydrolysis of n-dodecyl benzyl chloride with hydrothermal conditions was successful. The optimum process conditions were as follows: dodecyl dimethyl benzyl ammonium chloride as phase transfer catalyst, alkaline hydrothermal reaction at 130 鈩，
本文编号：2143734
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