水基钻井液抗高温降失水剂的制备与性能研究
发布时间：2018-10-20 12:50
【摘要】：随着浅部地层油气资源的日益枯竭,石油开采已逐步向深部地层发展,钻井液作为石油钻井作业中的重要组成部分,其高温稳定性直接决定钻井工程的成败。而钻井液处理剂的抗温耐盐性却是目前面临的一项重大技术难题,因此研制新型、廉价、性能优异的抗高温水基钻井液处理剂具有重要的理论和实际意义。 本文根据抗高温钻井液处理剂的分子结构设计的要求,优选了2-丙烯酰胺基-2-甲基丙磺酸(AMPS)、丙烯酰胺(AM)、二甲基二烯丙基氯化铵(DMDAAC)和对苯乙烯磺酸钠(SSS)为结构单体,采用过硫酸铵为引发剂,通过水溶液自由基聚合法合成出一种新型耐温共聚物降失水剂。通过单因素和正交实验对聚合反应条件进行优化,得到了合成AMPS/AM/DMDAAC/SSS四元共聚物的最优合成条件：单体总浓度(质量分数)=30%,单体配比n(AMPS):n(AM):n(DMDAAC):n(SSS)=5：7:2:1,引发剂加量(单体总质量的百分比)=0.8%,反应温度=75℃,pH=10,反应时间=6h。结合红外光谱(FTIR)、核磁共振氢谱(H1NMR)、热重(TGA)、DSC等分析方法对共聚物进行表征,结果表明四元共聚物AMPS/AM/DMDAAC/SSS含有所设计官能团,分子结构合理,且具有良好的热稳定性。 通过流变和滤失实验对AMPS/AM/DMDAAC/SSS四元共聚物性能进行评价,结果表明：此共聚物水溶液具有典型高聚物稀溶液特点,流变曲线符合幂率模式,粘度曲线具有剪切稀释性；共聚物在淡水基钻井液、4%盐水基钻井液和饱和盐水钻井液体系中均有较好的抗高温降滤失能力。由抗温和对比实验可知,AMPS/AM/DMDAAC/SSS四元共聚物具有较强的抗温耐盐降滤失能力,相同条件下性能明显优于AMPS/AM/NVP/SSS、SMP-Ⅱ和PAC-142。 通过复配实验,对各种处理剂进行优选及最佳用量的确定,获得了一个抗高温水基钻井液体系配方：4%土浆+0.2%FA-367+0.2%XY-27+2.0%SMP+3.0%SPNH+3.0%AM/AMPS/DMDAAC/SSS+重晶石粉。结果表明,该配方具有较好的抗高温降滤失作用且可控制老化180℃16h后体系的FL(API)在2mL左右,FL(HTHP)在9mL左右,符合抗高温水基钻井液体系设计要求。 最后,通过粒径分析和Zeta电位对共聚物的作用机理进行简要分析与讨论,结果表明,共聚物的加入能显著改善钻井液体系粘土颗粒的粒径大小和分布,有效促进粘土颗粒的水化分散能力,抑制粘土颗粒的聚结作用,通过粘土颗粒的紧密堆积形成致密的滤饼,从而达到降低滤失量的目的。
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【学位授予单位】：西南石油大学
【学位级别】：硕士
【学位授予年份】：2015
【分类号】：TE254.4
本文编号：2283244
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【学位授予单位】：西南石油大学
【学位级别】：硕士
【学位授予年份】：2015
【分类号】：TE254.4
【参考文献】
相关期刊论文 前10条
1 王力;万涛;王娟;孙自顺;张海波;熊磊;;淀粉接枝AM/SSS/DAC降滤失剂的制备与性能[J];广州化工;2012年02期
2 朱长豹;;深井超深井钻井技术现状和发展趋势[J];化工管理;2014年24期
3 江卫东,何国军,吴锰;高温抗盐降滤失剂SPX树脂的合成与评价[J];江汉石油学院学报;2001年01期
4 王中华;;P(AMPS-DMAM)共聚物钻井液降滤失剂的合成[J];精细与专用化学品;2010年07期
5 王中华;;P(AMPS-AM-AOETAC-AA)聚合物钻井液防塌降滤失剂的合成[J];精细与专用化学品;2010年10期
6 王中华;AM/AMPS/MAA/DADMAC四元共聚物的合成与性能[J];精细石油化工进展;2001年04期
7 王中华;AM/AA/淀粉接枝共聚物降滤失剂的合成及性能[J];精细石油化工进展;2003年02期
8 张高波,张希红,郭民乐;两性磺化酚醛树脂ASP-1的研制及性能评价[J];精细石油化工进展;2004年08期
9 陈晓飞;鲁红升;郭斐;李国成;黄志宇;;耐高温钻井液降滤失剂的研究[J];精细石油化工进展;2012年01期
10 鲍允纪;何跃超;孙立芹;张文郁;;酚脲醛树脂改性褐煤降滤失剂的合成与评价[J];精细石油化工;2011年05期
，本文编号：2283244
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