磷锗锌多晶合成装置设计研究

发布时间：2018-05-13 02:03

本文选题：磷锗锌 + 合成装置　；参考：《科学技术与工程》2016年05期

【摘要】：研究设计了ZnGeP_2多晶的合成装置,包括合成安瓿,合成炉结构与温场分布。利用自行设计的合成装置,采用两温区气相输运法进行ZnGeP_2多晶合成实验,并对合成的多晶材料进行XRD,EDS和密度测试。结果表明,合成产物为高纯、单相的ZnGeP_2多晶材料,设计的多晶合成装置和两温区气相输运合成工艺适合ZnGeP_2多晶的合成,为高质量ZnGeP_2多晶材料的获得奠定了基础。
[Abstract]:The synthesis device of ZnGeP_2 polycrystal, including ampoule synthesis, structure of synthesis furnace and temperature field distribution, was designed and studied. The ZnGeP_2 polycrystalline synthesis experiment was carried out by using the two-temperature vapor transport method with a self-designed synthesis device. The synthesized polycrystalline materials were tested by XRD-EDS and density. The results show that the synthesized products are high purity and single phase ZnGeP_2 polycrystalline materials. The designed polycrystalline synthesis device and two-temperature gas phase transport synthesis process are suitable for the synthesis of ZnGeP_2 polycrystals, which lays a foundation for obtaining high quality ZnGeP_2 polycrystalline materials.
【作者单位】：中国民用航空飞行学院;
【基金】：国家自然科学基金(50732005) 四川省科技厅基金项目(2015ZR0034) 中国民用航空飞行学院科研基金项目(J2014-92,Q2012-126)资助
【分类号】：TQ132.41

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