一款小角X射线散射原位测量专用简易样品加热装置

发布时间：2019-01-09 14:10

【摘要】：原位加热实验是同步辐射小角X射线散射领域的新热点。本文针对同步辐射小角X射线散射中需要加热并原位实时检测的实验而设计的一款样品简易原位加热专用装置,该装置主要由温控器、样品池、固定架组成,它具有结构简单、操作容易的特点。本文介绍该装置的基本结构、特点并采用该装置进行原位加热干燥褐煤实验,通过分析实验结果验证装置的可行性。
[Abstract]:In-situ heating experiment is a new hotspot in the field of small angle synchrotron radiation X-ray scattering. In this paper, a simple in situ heating device for synchrotron radiation in small angle X-ray scattering is designed. The device is mainly composed of a thermostat, a sample pool and a fixed frame. It has a simple structure. Features of ease of operation. In this paper, the basic structure and characteristics of the device are introduced, and the feasibility of the device is verified by analyzing the experimental results of in-situ heating and drying of lignite.
【作者单位】：安徽大学;北京同步辐射装置中国科学院高能物理研究所;
【基金】：研究生学术创新项目研究(yqh100207) 国家自然科学基金(U1332107、U1532105) 中国矿业大学(北京)煤炭资源与安全开采国家重点实验室开放课题(SKLCRSM14KFA02)
【分类号】：O434.1

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