农业院校研究生创新实验项目的设计与实践

发布时间：2018-04-13 23:21

本文选题：农业院校 + 化学工程与技术学科　；参考：《实验室研究与探索》2017年01期

【摘要】：根据农业院校化学工程与技术学科研究生的生源情况和专业特点,设计了一个创新实验项目。以异喹啉和六水氯化钴为原料,在含有浓盐酸的甲醇溶液中制备了四氯合钴(II)酸异喹啉盐杂化材料.用元素分析、X-射线衍射等手段表征了其组成和结构,研究了其红外光谱、紫外-可见光谱和磁学性能。实践表明,该实验项目原料易得,合成步骤简单,涵盖有机化学、配位化学、分析化学、晶体化学和分子磁化学等诸多知识点,具有一定的研究性和学术性,有利于培养研究生的创新能力和科学研究的能力。
[Abstract]:According to the situation of graduate students of chemical engineering and technology in agricultural colleges and the characteristics of their specialties, an innovative experimental project was designed.Isoquinoline salt hybrid material was prepared from isoquinoline and cobalt chloride hexahydrate in methanol solution containing concentrated hydrochloric acid.Its composition and structure were characterized by elemental analysis and X-ray diffraction. The infrared spectra, UV-Vis spectra and magnetic properties were studied.Practice shows that the experimental project is easy to obtain raw materials, simple synthesis steps, including organic chemistry, coordination chemistry, analytical chemistry, crystal chemistry and molecular magnetization and many other knowledge points, with a certain degree of research and academic,It is beneficial to cultivate the innovation ability of graduate students and the ability of scientific research.
【作者单位】：华南农业大学材料与能源学院化学实验教学中心;
【基金】：广东省科技计划项目(2014A010105037) 广东省研究生教育创新计划项目(2015SFKC08) 广东省教学质量工程项目(粤教高函[2014]97号),应用化学专业实验教学团队(粤教高函[2015]133号)
【分类号】：TQ0-4;G643

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